NEW DESIGN OF FLOW INJECTION ANALYSIS UNIT USING ( CE4++ I-+ H3O+) SYSTEM FOR THE DETERMINATION OF CERIUM(IV) BY MERGING ZONE TECHNIQUE . | ||
| Journal of University of Anbar for Pure Science | ||
| Article 14, Volume 7, Issue 2, August 2013, Pages 1-11 PDF (1.05 M) | ||
| Document Type: Research Paper | ||
| DOI: 10.37652/juaps.2013.84887 | ||
| Authors | ||
| DAKHEEL .N.TAHA1; FIRAS FADHEL ALI* 2 | ||
| 1University of Babylon - College of Science | ||
| 2Anbar University - College of Education for Girls | ||
| Abstract | ||
| The aim of this work was to design a new flow injection analysis unit for the determination of cerium(IV) by the reaction of potassium iodide with Ce4+ in an acidic medium to released I2 which have yellow color and give a λmax in 351 nm. The method involves the design of a new valve from cheap material and select the best design for unit .The optimum condition such as acid concentration , flow rate, potassium iodide concentration, acid volume, sample volume, reaction coil length, and interference effects were studied. Beer's law is obeyed over concentration rang (1- 40 mg/l), correlation coefficient(R2) was 0.998. | ||
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