Uncatalyzed thermal synthesis of new 1,2,3- triazole derivaties | ||
| Journal of Basrah Researches (Sciences) | ||
| Article 1, Volume 40, Issue 1, March 2014, Pages 146-159 PDF (0 K) | ||
| Author | ||
| Faeza Al-mashal and Nazik Hameed | ||
| Abstract | ||
| Two of new Azide and two of new 1,2,3-triazole compounds were synthesized. The triazole compound was prepared by 1,3-dipolar cycloaddition reaction of azido sulfacetmide and azido sulfamethazin with acetylene dicarboxylic acid in acetone as a solvents under reflux condition without catylest. The reaction mixture was followed by TLC and the yields of products following columgromotography. IR, H-NMR and Mass spectroscopes were used for the identification of prepared compounds | ||
| Keywords | ||
| Azides; Triazole; dipolar cycloaddition reactions | ||
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