Preparation Of New 2-Iminohexahydro-1,3-Thiazepine Derivatives | ||
| Al-Mustansiriyah Journal of Science | ||
| Article 1, Volume 23, Issue 6, September 2012, Pages 93-116 | ||
| Author | ||
| Hamed Jassim Jaffar | ||
| Abstract | ||
| A new 2-iminohexahydro-1,3-thiazepine derivatives were synthesized from cyclo condensation of thiourea derivatives with 1,4- dibromobutane in presence of NaH as reducing agent . Acid chlorides were used with primary amine as convenient starting materials for synthesis of (33) thiourea derivatives . The synthesized compounds were characterized by different spectroscopic methods (FTIR,1H-NMR). | ||
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