Synthesis of New Derivative of Adipoyl Thiadiazole | ||
| Tikrit Journal of Pure Science | ||
| Article 1, Volume 17, Issue 2, June 2012, Pages 127-132 | ||
| Authors | ||
| Entesar O. Al; ; Enaam Fadil Mousa | ||
| Abstract | ||
| This research includes the preparation of new derivatives of adipoyl thiadiazoles, through the reaction of each of hydrazine hydrate , phenyl hydrazine , 2,4-dinitrophenyl hydrazine, semicarbazide and thiosemicarbazid with adipoly chloride in the presence of ethanol (95%). Furthermore, thiadiazoles were made through cyclization of hydrazine , semicarbazide and thiosemicarbazid in alkaline media, such as potassium hydroxide solution in presence of carbon disulfide. The prepared compounds were identified by the physical and spectroscopic methods | ||
| Keywords | ||
| thiadiazole; hydrizides; semicarbazide; Thiosemicarbazide; adipoly chloride; Carbon disulfide | ||
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