Structure and Optical properties of Lead Sulfide (PbS) Thin Film Prepared by Chemical Bath Deposition(CBD) Technique: A Review

Ali, Ghazwan Ghazi; Aswad, Tahseen Ali

doi:10.37652/juaps.2023.181569

	Structure and Optical properties of Lead Sulfide (PbS) Thin Film Prepared by Chemical Bath Deposition(CBD) Technique: A Review
Journal of University of Anbar for Pure Science
Article 31, Volume 17, Issue 2, December 2023, Pages 225-233 PDF (695.5 K)
Document Type: Review Paper
DOI: 10.37652/juaps.2023.181569
Authors
Ghazwan Ghazi Ali^* ¹; Tahseen Ali Aswad²
¹Physics Department, College of Education for Pure Science, Mosul University,Mosul, Iraq;
²The Directorate General of Education in Salah al Din,
Abstract
In this review, the chemical bath deposition method has been studied to investigate lead sulfide thin film. The important results obtained from XRD, AFM and optical Spectrophotometer measurements were discussed. peaks patterns illustrated that the lead sulfide structure have a cubic phase nanocrystalline corresponded to the strong peaks (111) and (200) at 2θ ≅ 26.3^◦ and 29.8^◦ respectively. Atomic force microscope (AFM) images exhibited that the lead sulfide (PbS) thin films have a nano-size grain also the grain size increased with increasing film thickness. Different parameters such as dislocation density and internal strain have been studied to be decreased with concentration. Decreasing internal strain and dislocation density with increasing concentration show enhancement of lattice constant as prepared films Scanning electron Microscope (SEM) images displayed that the top surface layers are strongly affected depending on the nature top. The PbS structure are quite homogeneous , the size distribution was about 71–83 nm. The influence of deposition time, thickness, nature of the substrate, concentration of solution and doping on the PbS films was also discussed. It can be seen, The prepared thin film was a thinner film with a short deposition time compared to prepared samples with a longer time. It has also been found that the precipitated films show optical absorbance in the room and UV region but their absorbance decreases upon entering the near-infrared (NIR) region. Lead Sulfide thin films have gained remarkable attention worldwide due to an important narrow band gap semiconductor which has broad potential applications in optoelectronics devices.
Keywords
Thin Film; Chemical Bath Deposition; Lead Sulfide; Structural and Optical Properties
Supplementary Files 30 (no, 2 , Vol,17 )2023.docx
References
[1] Duan, T., Lou,W., Wang, X. and Xue, Q. (2007). ″Size-controlled synthesis of orderly organized cube-shaped lead sulfide nanocrystals via a solvothermal single source precursor method″, Colloids and Surfaces A: Physicochemical and Engineering Aspects, 310, 86-93. [2]Mitesh, H. P. , Tapas, K. C. , Vaibhav, K. P. (2017). Shripathi, T. , Deshpande, U. & Lalla, N. P , Dip-coated PbS/PVP nanocomposite films with tunable band gap, RSC Adv., 63(7) 4422-4429. [3] Defa, W., Jayanta, K. B. , Haiguang, Z. , Belete, A. G., Vo-Van, T., My Ali, E. K., Ricardo, I. & Dongling, M. (2011). Controlled fabrication of PbS quantum-dot /carbon nanotube nanoarchitecture and its significant contribution to near infrared photon-to-current conversion, Adv. Funct. Mater., 21, 4010–4018. [4] Bai, R. , Kumar, D. , Chaudhary, S. & Pandya, D. K. (2017). Highly crystalline p- PbS thin flms with tunable optical and hole transport parameters by chemical bath deposition, Acta Mater.,131, 11-21. [5] Moreno, O. P. , Lima, L. A. C. , Portillo, M. C. , Castilla, S. R. , Tototzintle, M. Z. , Avila, G. A. & Perez, R. G. (2012). Properties of PbS:Ni²⁺ nanocrystals in thin flms by chemical bath deposition, ISRN Nanotechnol.,1–13 DOI: 10.5402/2012/546027. [6] Ahmed, A. M. , Rabia, M. & Shaban, M. (2020). The structure and photoelectro- chemical activity of Cr-doped PbS thin films grown by chemical bath deposition. The Royal Society of Chemistry, 10(24), 14458–14470. [7]Hern´andez-Borja, J., Vorobiev, Y. V. & Ram´ırez-Bon, R. (2011). Thin film solar cells of CdS/PbS chemically deposited by an ammonia-free process. Solar Energy Materials and Solar Cells, 95, (7) 1882-1888. [8]Ghamsari, M. S. , Araghi, M. K. & Farahani, S. J.(2006). The influence of hydrazine hydrate on the photoconductivity of PbS thin film. Materials Science and Engineering: B, 133, (1-3), 113–116. [9]Gunes, S. , Fritz, K. P. , Neugebauer, H. , Sariciftci, N. S. , Kumar, S. & Scholes, G. D. (2007). Hybrid solar cells using PbS nanoparticles. Solar Energy Materials and Solar Cells, 91,(5) 420-423. [10]Enue, B., Rodrguez, Y., Juan, P. P., Colin, J., Altuzar, P., Campos, J. & David, Q. (2019). Effect of Deposition Time on the Optoelectronics Properties of PbS Thin Films Obtained by Microwave-Assisted Chemical Bath Deposition. Advances in Condensed Matter Physics, 8 pages, DOI: 10.1155/2019/5960587. [11]Abdallah, B. , Hussein, R. , Al-Kafri, N. & Zetoun, W. (2019). PbS Thin Films Prepared by Chemical Bath Deposition:Effects of Concentration on the Morphology, Structure and Optical Properties. Iranian Journal of Science and Technology, Transactions A: Science, 43, pages1371–1380. [12]Ho Soonmin, A. K. & Tan, W. (2014). Chemical Bath Deposited Lead Sulphide Thin Films: Preparation and Characterization. World of Mechanics,1 (1), 1-6. [13]Tusamalee, P., Buranasiri, P., Chaisitsak, S. & Yindeesuk, W. (2017). Optical Properties of PbS Thin Films Prepared by Successive Ionic Layer Adsorption and Reaction Processes. Journal of Materials Science and Applied Energy, 6(3), 211- 214. [14]Aadim, K. A. Ibrahim, A. E. & Marie, J. M. (2017). Structural and Optical Properties of PbS Thin Films Deposited by Pulsed Laser Deposited (PLD) Technique at Different Annealing Temperature. International Journal of Physics, 5(1), 1-8. [15]Ubale, A.U. , Junchara, A.R. , Wadibhasme, N.H. , Darya Purkab, A.S. , Mankar, R.B. & Sangawar, V.S. (2007). Thickness dependent structural, electrical and optical properties of chemically deposited nano particle PbS thin film, Turk. J. Phys, 31, 279-286. [16]Kumar, R. & Das, R. (2014). Optical and Electrical Characterization of Nano- crystalline (Pb_{1- X}bi) S Thin Films Deposited at Room Temprature. IOSR Journal of Applied Physics, e-ISSN: 2278-4861, PP 07-10. [17]Nascu, C. , Vomir, V. , Pop, I. , Ionescu, V. & Grecu, R. (1996). The study of lead sulphide films.VI. Influence of oxidants on the chemically deposited PbS thin films , Mater. Sci. Eng. B. 841, 235-240. [18]Machol, J.L. , Wise, F.W. , Patel, R.C. & Tanner, D.B. (1993). Vibronic quantum beats in PbS microcrystallites Phys. Rev. B., 48, 2819- 2822. [19]Nayak, B.B. & Acharya, H.N. (1985). Characterization of chemically deposited Pb1-x CdxS films by scanning electron microscopy, J. Mater. Sci. Lett.4, 651-652. [20]Thangaraju, B. & Kaliannan, P. (2000). Polycrystalline lead tin chalcogenide thin film grown by spray pyrolysis, Cryst. Res. Technol. 35(1), 71-75. [21]Nair, P.K. , Garcia, V. M. , Hernandez, A.B. & Nair, M.T.S.(1991). Photoacceler-ated chemical deposition of PbS thin films: novel applications in decorative coat-ings and imaging techniques. J. Phys. D: Appl. Phys. 24, 1466-1472. [22]Pop, I. , Nascu, C. , Ionescu, V. , Indrea, E. & Bratu, I. (1997). Structural and optical properties of PbS thin films obtained by chemical deposition, Thin Solid Films 307, 240–244. [23]Malyarevich, A. M. , Gaponenko, M. S. , Savitski, V. G. , Yumashev, K. V. , Rachkovskaya, G. E. & Zakharevich, G. B. (2007). Nonlinear optical properties of PbS quantum dots in borosilicate glass, Journal of Non-Crystalline Solids, 353, (11-12), 1195–1200. [24] Ezekoye, B. A. , Emeakaroha, T. M. , Ezekoye, V. A. , Ighodalo, K. O. & Offor, P. O. (2015). Optical and structural properties of lead sulfide (PbS) thin films synthesized by chemical method. International Journal of Physical Sciences,10 (13), 385-390. [25] Gülen, Y. (2014). Characteristics of Ba-Doped PbS Thin Films Prepared by the SILAR Method. Acta Physica Polonica A. 126, 763-767. [26] Puišo, J. , Lindroos, S. , Tamulevicius, S. , Leskelä, M, , Snitka, V. (2003).The influence of the pretreatment of Si substrate on the growth of PbS thin films in the SILAR Technique. Solid State Phenomena, 94, 261- 264. [27] Sarma, M.P. & Wary, G. (2017). Effect of Molarity on Structural and Optical Properties of Chemically Deposited Nanocrystalline PbS Thin Film. Internation- al Letters of Chemistry, Physics and Astronomy, 74, 22-35. [28] Thangaraju, B. , Kalainnan, P. (2000). Spray pyrolytically deposited PbS thin films, Semicond. Sci. Technol. 15 , 849–853. [29] Mondal, A. , Mukherjee, N. (2006). Cubic PbS thin films on TCO glass substrate by galvanic technique. Mater Lett, 60, 2672-2674. [30]Sharon, M. , Ramaiah, K.S. , kumar, M. , Neumann-Spallart, M. & Levy Clement, C. (1997). Electrodeposition of lead sulphide in acidic medium,Journal of Electroanalytical Chemistry. 436 (1-2), 49-52. [31]Ge, J. P. , Wang, J. , Zhang, H. X. , Wang, X. , Peng, Q. & Li, Y. D. (2005). Orthogonal PbS nanowire arrays and networks and their raman scattering behavior, Chrmistry A European Journal, 11,(6) 1889-1894. [32]Dawood, Y. Z. , Kadhim, S. M. & Mohammed, A. Z. (2015). Structure and optical properties of nano PbS thin film deposited by pulse laser deposition, Eng & Tech Journal,. Part (B), 32, 1723–1730. [33]Koao, L. F. , Hone, F. G. & Dejene, F. B. (2020). Synthesis and characterization of PbS nanowires doped with Tb³⁺ions by using chemical bath deposition method. Journal of Nanostructure in Chemistry, 10,1–7. [34]Saraidarov, T. , Reisfed, R. , Sashchiuk, A. , Lifshitz, E. (2005). Nanocrystallites of lead sulfide in hybrid films prepared by sol-gel process. J. Sol-Gel Sci.Technol. 34, 137–145. [35]Oriaku, C.I. & Osuwa, J.C. (2008). Analysis of thin chalcogenide PbS films prepared from chemical path, The Specific Journals of science and technology, 9 (2), 461-467. [36]Busarin, N. , Panita, C. ,Intira, S. & Chanwit, C. (2008). The Influence of Growth Conditions on the Chemical Bath Deposited ZnS Thin Films. Journal of Metals, Materials and Minerals, 18 (2 ) , 49-52. [37]Cheemadan, S. , Keerthana, K. & Santhosh Kumar, M. C. (2013). Analysis of Structural and Electrical Properties of Aluminium Doped Lead Sulphide (PbS) Thin Films Prepared by CBD Method. J. Environ. Nanotechnol., 2(4), 28-33. [38]Olabisi, O. & Adegboyega, O., (2018). Optical and Microstructural Analysis of Chemically prepared Lead Sulphide (PbS) Thin Film. International Journal of Trend in Scientific Research and Development, 2(2), 1006-1008. [39]Kavitha, C. , Gopinathan, C. & Pandi, P. (2017). Lead Sulfide (PbS) Thin Film with Different Thiourea Concentrations. Journal of Nanoscience and Technology , 3(3), 284–288. [40]Ramalan, A.M. , Yusuf, A.S. , Samson, D.O. & Buba, A.D. (2018). Optical, Morphological and Electrical Properties of PBS Thin Films Prepared by Chemical Bath Deposition (CBD) Technique at Different Deposition Time. American Based Research Journal, 7(11), 1-8. [41]Raghumani, S. L. , Nabachandra, S. A. , Nabadwip, S. S. & Bidyaswor, S. S., (2018). Structural Characterization of PbS and Cd-doped PbS Nanocrystalline Thin Film Fabricated By Chemical Bath Deposition Technique. International Journal of Innovative Research in Science, Engineering and Technology,7(1), 537-541. [42]Seghaier, S. , Kamoun, N. , Brini, R. & Amara, A.B. (2006). Structural and optical properties of PbS thin films deposited by chemical bath deposition. Materials Chemistry and Physics, 97, 71–80. [43]Abass, M., Al-Fawadi, E.& Al-Samuraee, A. K.(2009). Preparation of Nanocry-stalline PbS Thin Films by Chemical Bath Deposition. Materials Science and Technology, October 25-29 , 2637-2646. [44]Obaid, A.S. , Mahdi, M. A. , Dihe, A. A. & Hassan, Z. (2012). Effect of Depositi- on Time on the PbS Thin films Prepared using Microwave-Assisted Chemical Bath Deposition: Structure and Optical Characterization. International Conference on Education, Applied Sciences and Management, December 26-27, 86-89. [45]Palomino, M. R. , Portillo, M. O. , Chaltel, L. A. , Gutiérrez, P. R. , Icaza, H. M. & Castaño, V. M. (2013). Chemical Bath Deposition of PbS:Hg²⁺ Nanocrysta- lline Thin Films. Journal of Nanomaterials, Research Article, 6 pages. [46]Göde, F. , Yavuz, F. and Kariper, I.A. ″Preparation and Characterization of Nanocrystalline PbS Thin Films Produced by Chemical Bath Deposition″. Acta Physica Polonica A, 128,2, 215-218, (2015). [47]Aye, M. M. , Win, H. H. & Aung, M. T. (2017). Nanocrystalline lead sulphide thin films fabrication and characterization. International Research Journal of Advanced Engineering and Science, 2(3), 257-260. [48]Rajathi, S. , Kirubavathi, K. & Selvaraju, K. (2017). Preparation of nanocrystal- line Cd-doped PbS thin films and their structural and optical properties. Journal of Taibah University for Science, 11, 1296–1305. [49]Abdallah, B. , Ismail, A. , Kashoua, H. & Zetoun, W. (2018). Effects of Deposition Time on the Morphology, Structure, and Optical Properties of PbS Thin Films Prepared by Chemical Bath Deposition. Journal of Nanomaterials, Research Article, 8 pages. [50]Horoz, S. , Ekinci, A. & Sahin, O. (2018). Synthesis of PbS and Ni-doped PbS thin films by CBD method and investigation of their structural, optical and photovoltaic properties. Journal of Ovonic Research, 14(3), 201 – 208. [51]Manouchehri, S. , Zahmatkesh, J. & Yousefi, M. H. (2018). Substrate Effects on the Structural Properties of Thin Films of Lead Sulfide. Journal of Optoelectron- ical Nanostructures, 3(2), 1-18.
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