Synthesis of Vanadium Pentoxide using Hydrothermal Autoclave Approach | ||
| Journal of University of Anbar for Pure Science | ||
| Article 13, Volume 17, Issue 2, December 2023, Pages 81-85 PDF (603.9 K) | ||
| Document Type: Research Paper | ||
| DOI: 10.37652/juaps.2023.140257.1070 | ||
| Authors | ||
| Amal Shakir Abbood* 1; Ibraheem Jaleel Ibraheem2 | ||
| 1College of Dentistry, University of Anbar ,Ramadi, Iraq; | ||
| 2Department of Chemistry, College of Science, University of Anbar, Al-anbar, Iraq. | ||
| Abstract | ||
| The transition metal vanadium can easily move between the oxidation states +V, +IV, and +III and expand its sphere beyond tetrahedral coordination. It oxidizes into a brownish black trioxide, a blue-black tetroxide, or a reddish orange pentoxide when heated in air at various temperatures. The simple hydrothermal autoclave approach was used to synthesize vanadium pentoxide V2O5 nanoparticles from ammonium metavanadate NH4VO3. The synthesized sample was identification using X-Ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and atomic force microscopy (AFM). The result confirms forming of V2O5 nanoparticles and the diameter was around 61- 167 nm. The transition metal vanadium can easily move between the oxidation states +V, +IV, and +III and expand its sphere beyond tetrahedral coordination. It oxidizes into a brownish black trioxide, a blue-black tetroxide, or a reddish orange pentoxide when heated in air at various temperatures. The simple hydrothermal autoclave approach was used to synthesize vanadium pentoxide V2O5 nanoparticles from ammonium metavanadate NH4VO3. The synthesized sample was identification using X-Ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and atomic force microscopy (AFM). The result confirms forming of V2O5 nanoparticles and the diameter was around 61- 167 nm. | ||
| Keywords | ||
| Hydrothermal,,; ,،Metal oxide,,; ,،Nanoparticles,,; ,،V2O5 | ||
| References | ||
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