Preparation of Al2O3/MgO Nano-Composite Particles for Bio-Applications | ||
| Engineering and Technology Journal | ||
| Article 12, Volume 38, 4A, April 2020, Pages 586-593 PDF (723.56 K) | ||
| DOI: 10.30684/etj.v38i4A.290 | ||
| Authors | ||
| Hayder A. Sallal* 1; Alla A. Abdul-Hameed2; Farhad. M. Othman1 | ||
| 1Materials Engineering Department, University of Technology, Baghdad, Iraq | ||
| 2Materials Engineering Department, University of Technology, Baghdad, Iraq. | ||
| Abstract | ||
| This study describes the preparation and study of the properties of Nano composite particles prepared in a sol-gel method which consists of two materials (Αl2Ο3-MgΟ). The powder was evaluated by x-ray diffraction analysis, scanning electron microscopy analysis (SEM), particle size analysis, and energy dispersive x-ray analysis (EDX) and antibacterial test. The evaluation results of the nanocomposite particles shows a good distribution of the chemical composition between aluminum oxide and magnesium oxide, smoothness in particles size where it reached to (54.9, 59.8) nm at calcination in (550 0C and 850 0C) respectively, formation of different shapes of nanoparticles and different phases of the Αl2Ο3 particles (kappa and gamma) and nanopowder have well antibacterial action, Therefore, this reflects the efficiency of the proposed method to manufacture the nanocomposite powder and the possibility of using this powder as a strengthening material for the composite materials and using these composite materials in bio applications, especially in the fabrication of artificial limbs. | ||
| Keywords | ||
| Nano composite particles; sol-gel method; bio Applications | ||
| References | ||
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[1] J. Li, “Nanostructured biomaterials,” Zhеjiang University Press, 1st Edition, Hangzhou and Springer-Verlag Berlin Heidelberg, 2009. [2] Q. Zhang, L. Si Xu , X. Guo, “Improvements of mechanical properties, microscopic structures, and antibacterial activity by Ag/ZnO nano composite powder for glaze-decorated ceramic,” Journal of Advanced Ceramics, Vol.6 , No.3, pp.269–278, 2017. [3] P. Ajayan and L. Schadler, “Nano composite science and technology,” Weinheim: WILEY-VCH Verlag GmbH & Co. KGaA, 2003. [4] M. John ,”Nanotechnology 101,” Greenwood Press, 1st Edition, Greenwood Publishing Group, London, 2007. [5] M. Shams, Z. Ahmadi and S. Hydari, “Synthesis and characterization of nanowires zinc oxide with different temperatures,” Journal of Chemical Engineering , Vol. 41, No. 4, pp.191 – 201, 2013. [6] H. Ding, G. Zhou, Y. Zhang,” Fretting tribology of Αl2Ο3/Сu composites prepared by powder metallurgy,” Materials Sciences Forum, Trans Tech Publications, Vol.12, No.5, 2009. [7] R. A. Ilyas, S. M. Sapuan , M. R. Ishak, E. S . Ilyas, “Effect of delignification on the physical, thermal, chemical, and structural properties of sugar palm fiber,” Bio Resources Journal, Vol. 12, No.4, pp.8734-8754, 2018. [8] H. Abral., A. Basri , F. Μuhammad, Y. Fernando, F. Hafizulhaq, M. Mahardika , S. Eni .Sapuan, R. A.Ilyas, “Simple methods for improving the properties' of the sago starch films prepared by using ultra sonication treatments,” Journal Food Hydrocolloids; Vol. 93, No.4, pp.276-283, 2019. [9] R. A. Ilyas , S. M. Sampan , M. L. Samyang, M.R. Ishakc, E.S. Zainudin, “Nano crystalline cellulose as reinforcement for polymeric matrix nano composites and its potential applications: a review ,” Current Analytical Chemistry Journal, Vol.14, 2019. [10] M. Di.Ventra and S. Envoy, “Introduction to nano scale science and technology,” Emerald, 1st Edition, England Chp.1, 2004. [11] A. Besinis and T. De Peralta, “Review of nanomaterial's in dentistry: interactions with the oral microenvironments, clinical applications', hazards, and benefits,” American Chemical Society, Vol. 9 , No. 2, pp.2255-2289, 2015. [12] Sanjay. G, “Sol-gel synthesis of titanium dioxide,” Springer, 1st Edition, Germany, 2017. [13] A. Crestian, C. Monro, T. Velagio, C. Logan, “ZnO-SiO2 based nano composites prepared by a modified sol-gel methods,” Materials Chemistry and Physics, Vol.186, pp.399-406, 2019. [14] Μ. S. WAGH, A. M. PATIL,֛ ” Preparation of MgO nanostructures powder by sol-gel methods,” Internationals Journal of chemicals and Physical Sciences' IJCPS Vol. 4 , No.7 pp.291 – 300, 2015. [15] Z. X. Tang, B. Feng Lv, “MgO nanoparticles' as antimicrobials agent: preparations and activity,” by Brazilian Journals of chemicals engineering, Vol. 31, No. 03, pp.591 - 601, July – Septembers, 2014. [16] C. Ruberto, “Bulk and surface structure of alumina,” Thesis of Department of Applied Physics, Chalmers University of Technology and Goteborg University, 1998. [17] S. J. Mosaic, Μ. R. Abolhassani, S. M. Hosseini, and Ѕ. A. Sebt, “Comparison of electronica and optical properties' of the phases of alumina using density functional theory,” Chinese Journal of Physics, Vol. 47,No. 6, 2009. [18] H. Ding G. Zhou, Y. Zhang, “Fretting tribology of Al2O3/Cu composite prepared by powder metallurgy,” Materials Science Forum, Trans Tech Publications, Switzerland, Vol. 21, No. 5, pp.91 – 111, 2009 [19] E. Q. Arther, A.B. Thomas, K.R. Dany, “Nano-MgO particle size influence of on bactericidal action against multi bacteria ,” Bulletin Sciences, India, Vol.71, pp.633-821 , 2019. [20] C. J. Hewit , B. Shangen, A. Ahmadi , N. von Caron, and C. Mcfarlane, “An evaluation of the antibacterial action of ceramics powder slurries using multipara meter flow cytometers,” Biotechnology Letters Vol.23,pp.667-675 , 2001. | ||
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