Optical and Thermal Characterizations of PMMA Composites | ||
Engineering and Technology Journal | ||
Article 5, Volume 37, 2B, May 2019, Pages 61-66 PDF (1.32 M) | ||
DOI: 10.30684/etj.37.2B.5 | ||
Authors | ||
Raghad S. Al-Khafaji1; Kareem A. Jasim1; Adil M. Ibraheim2 | ||
1University of Baghdad College of EducationIbn - Al-Haithem, Department of Physics, Baghdad - Iraq | ||
2Ministry of Education Baghdad, Al-Rusafa 2, Baghdad - Iraq | ||
Abstract | ||
Thick composite films were prepared employing hand – layup method . A definite quantity of PMMA ( 98%wt ) , fixed content ( 2% wt ) of rutile titanium dioxide TiO2 , gamma alumina ( ᵞ- Al2O3 ) and Zirconia powder ( ZrO2 ) , were added to polymer solution gradually and separately. Optical constants were obtained of the prepared samples using spectrometer (UV- VIS). The prepared composite samples were thermally characterized by differential scanning calorimeter ( DSC ). We notice increasing value of glass temperature and differential heat capacity ( ∆Cp ) for composites compared with pure PMMA . | ||
Keywords | ||
Binary composite; PMMA; TiO2; Al2O3; ZrO2; Optical Constants; thermal analysis | ||
References | ||
[1].J. singh " Electronic and Optoelectronic properties of semiconductor structures " pp 364 , 2003 . [2].A. S.Ayesh " Electrical and Optical characterization of PMMA doped with y0.0025 , Si0.025 , Ba0.9725 ( Ti(0.9) Sn0.1 ) Q3 ceramic , chinese Journal of polymer science Vol.28 , No.4 , pp 537 – 546-2010 . [3].R. Boylestad and Louis Nashelsky " Electronic Devices and Circuit Theory" seventh edition pp 5-8 1999. [4].V.Raghavan " Materials Science and Engineering " fifth edition pp 356-360 , 2010 . [5].S.L.Rosen .Fundimental principles of polymeric materials , John Willey &Sons . Inc . Newyork , 1993 . [6].A. K.Kaw " Mechanics of compsite Materials " 2th edition , Taylor & Francis Group , 2006 . [7].J.Brandup , E.H.lmmergut and E.Grulk , " polymer Handbook " 4th edition , John Wiley , Newyork , 1999 . [8]. S. kalbandhe , Ankita Thikane and shubhashree munot " Pmma Nano – Composites" International conference on Ideas , Impact and Innovation in mechanical Engineering , V. 5 ,pp 1627-1632 , 2017 . [9]. B.S.Hayes and L.M.Gammon " Optical Microscopy of fiber-Reinforced composites " , ASM International , pp 17-22 , 2010 . [10]. D.Lukkassen and Annete Meidell " Advanced Materials and Structures and their Fabrication processes " book manuscript , Navvik university college , Hing , pp190-192 , 2007 . [11]. P.S.Kireev , " Semiconductor physics " , 2nd edition , Translated from The Russian by M.samokhvalov , Mir publishers Moscow , pp .16-331 , 1978 . [12]. S.Rani and J.shanthi " Effect of annealing on the optical transmittance behavior of electron beam evaporated CdSe thin films " international Journal of Recent Scientific Research , Vol .5 , pp 118 – 119 , 2014 [13]. M.A.Diab,,N.A.ALGhamaz , "conducting polymers VIII optical and electrical " polymer testing , Vol.63,pp440-447,201 [14]. S.Sun , Yu Wang ''In situ synthesis of poly nano composites and their optical properties '' springer , polymer science , vol. 59, pp 630-638 , 2017 [15].A.Ehsani , Shirin Adeli ''Electrochemical and optical properties of TIO2 nanoparticales / poly composites films '' journal of Electro analytical ''Vol . 713 , pp 91-97 ,2014 [16].S.M.Scholz, G.Carrot and J.Hilborn,”Opticalproperties of Gold-Containing Poly (Acrylic Acid) “,LausanneSwitzerland,(2008). | ||
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