Derivative UV-Spectroscopic Studies of some Schiff Bases in Absolute Ethanol | ||
Journal of Education and Science | ||
Article 15, Volume 28, Issue 2, June 2019, Pages 219-232 PDF (1.01 M) | ||
Document Type: Research Paper | ||
DOI: 10.33899/edusj.2019.161211 | ||
Author | ||
Amel G. gassy Abed | ||
Abstract | ||
According to the biological and industrail importance of Schiff bases compounds , a new simple and accurate UV spectrophotometric method was established for the studied and determination of the Schiff bases compounds formed from the reaction between aromatic aldehydes compounds and P-toluenesulphonamide , depending on the zero and fourth derivative mode techniques . The zeroth and fourth order derivative spectra of the Schiff bases : [benzylidine (compound I) , 3, 4 – dimethoxybenzylidine (compound II) and 2 ,6 – dichorobenzylidine (compound III)] p-toluenesulphonamid , were recorded in absolute ethanol for series of different concentration solutions . The calibration curves were ploted which result in astraight lines obeying Beers – Lambert law with R2 values and R.S.D for compound I . II and III . These values indicate that these techniques having good sensitivity and precision for the quantification of these Schiff bases . | ||
Keywords | ||
fourth order; Schiff base; p-toluenesulphonamid | ||
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