A study of condensation of propane-1,3Diamine with formaldehyde | ||
| Journal of University of Anbar for Pure Science | ||
| Article 9, Volume 3, Issue 3, December 2009, Pages 28-34 PDF (562.56 K) | ||
| Document Type: Research Paper | ||
| DOI: 10.37652/juaps.2009.15556 | ||
| Author | ||
| Ahmed H. Shukkur* | ||
| University of Anbar - College of Education for Pure Sciences | ||
| Abstract | ||
| The condensation of formaldehyde with propane-1,3-diamine gave four products depending on the conditions of the reaction of them dimer, trimer, tetramer and pentamer of N,N΄-bis(methylene)propane-1,3-diamine products (CH2=NCH2CH2CH2N=CH2). Their structures were determined by MS, elemental analysis and 1H NMR spectroscopy methods. The structure of the pentamer was additionally determined by X-ray diffraction analysis. | ||
| Keywords | ||
| Condensation; propane; diamine; Formaldehyde; ray diffraction analysis | ||
| References | ||
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[1]- Krassig H. (1956).// Makromol. Chem., Vol. 17, № 2, P. 77-89.
[2]- G. M. Sheldrick, SHELX-86, Program for the Solution of Crystal Structures, University of Göِttingen, Gِöttingen (Germany), 1993.
[3]- G. M. Sheldrick, SHELX-86, Program for the Refinement of Crystal Structures, University of Göِttingen, Göِttingen (Germany), 1993. | ||
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