Synthesis and Characterization of Novel1,3,4,9a-Tetrahydrobenzo[e][1,3]oxazepin-5(5aH)-one Derivativesvia Cycloaddition Reactions ofSchiff Bases | ||
| Journal of University of Anbar for Pure Science | ||
| Article 3, Volume 10, Issue 3, December 2016, Pages 8-18 PDF (1.09 M) | ||
| Document Type: Research Paper | ||
| DOI: 10.37652/juaps.2016.135150 | ||
| Authors | ||
| Obaid H. Abid* 1; Rasim F. Muslim2; Khalid M. Mohammed3 | ||
| 1University of Fallujah | ||
| 2University of Anbar - College of Applied Sciences-Heet | ||
| 3University of Tikrit - College of Education for Pure Sciences | ||
| Abstract | ||
| A series of novel1,3,4,9a-tetrahydrobenzo[e][1,3]oxazepin-5(5aH)-one derivatives were synthesized by the reaction of Schiff bases with bicyclo]2.2.2[oct.7-ene-2,3,5,6-tetracarboxylic anhydridein anhydrous acetonitrile under dry and reflux conditionswith high yields via polar cycloaddition. Schiff bases were synthesized by the reaction of aromatic aldehydes, ketones or preparedchalcones with primary aromatic amines. The products were identified by their melting point,FT-IR, UV-Vis-spectra, 1H-NMR and13C-NMR spectra. | ||
| Keywords | ||
| novel; tetrahydrobenzo; Schiff bases; reflux conditions | ||
| References | ||
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