Preparation and diagnosis some heterocyclic compounds that derived from 1,3,4 – Thiadiazole compound derived from 1,3,4 – Thiadiazole compound | ||
| Kirkuk Journal of Science | ||
| Article 1, Volume 11, Issue 4, December 2016, Pages 184-197 PDF (0 K) | ||
| DOI: 10.32894/kujss.2016.131072 | ||
| Author | ||
| Ayad S. H. AL-Maaini Nazhan.KA AL-Luhiby | ||
| Abstract | ||
| This search included synthesis of some heterocyclic compounds devired from 1,3,4- thiadiazol ring ,such as thaiazolidin -4-one substituents Azetidine -3- one and Azo dyes. These compounds were aprepard from Shiff bases loaded on thiazdiazol ring, These bases have been treated with Aniline substituents in presence of pyrididine as a catalyst to give azo dyes , thioglycolic acid to produce thiazolidine -4- one in presence of ZnCl2 as catalyst and finally with chloroacetylchloride to produce Azetidine-3-one in presence of tryethylamine as a catalyst. The prepared compounds were identifie by physical properties and IR,H1-NMR Spectroscopy. | ||
| Keywords | ||
| cyclic compounds; Heterocyclic; thiadiazole | ||
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