Synthesis, Characterization, and Antibacterial effect of Complexes lead(II) and Tin (II) With (L-leucin and 8-hydroxyquinoline) | ||
| journal of al-qadisiyah for pure science(quarterly) | ||
| Article 1, Volume 12, Issue 4, December 2012, Pages 104-112 PDF (0 K) | ||
| Author | ||
| Taghreed H. Al- Noor | ||
| Abstract | ||
| The research includes the synthesis and identification of two types complexes of M+2 Ions using amino acid( L-leucin) and 8-hydroxyqinoline as ligands in general compositions [ M (Leu)2] and [ M (Q)2] were L-leucin (C6H13NO2)symbolized as (LeuH), and 8-hydroxyqinoline,(C9H7NO2) symbolized as (8-HQ), M(II)= Sn(II) and Pb(II), The ligand and metal ions were brought into reaction in ethanolic medium using (1:2) metal : ligand molar ratios as required. Products were found to be solid crystalline complexes, which have been Characterized through the following techniques: Melting points, Solubility, Molar conductivity. Determination the percentage of the metal in the complexes by (Atomic Absorption Spectrometry). chloride ion content were also evolution by (mohr method) . Spectroscopic Methods [FT-IR and UV-Vis]. The proposed structure of the complexes using program , chem office 3D(2006) . | ||
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