M. Sarhan, B., of Education for Pure Sciences, C., of Education- Iraq, M., Ibn-AL-Haitham, , J. Waheed Department of Chemistry, E., of Baghdad Awf A.R. Ahmed Teacher, U. (2016). Synthesis and Characterization of Some Metal Complexes of [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1H-pyrazol-4-ylcarbamothioyl) benzamide]. Alustath, 22(96), 49-62.
Basima M. Sarhan; College of Education for Pure Sciences; Ministry of Education- Iraq; Ibn-AL-Haitham; Enass J. Waheed Department of Chemistry; University of Baghdad Awf A.R. Ahmed Teacher. "Synthesis and Characterization of Some Metal Complexes of [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1H-pyrazol-4-ylcarbamothioyl) benzamide]". Alustath, 22, 96, 2016, 49-62.
M. Sarhan, B., of Education for Pure Sciences, C., of Education- Iraq, M., Ibn-AL-Haitham, , J. Waheed Department of Chemistry, E., of Baghdad Awf A.R. Ahmed Teacher, U. (2016). 'Synthesis and Characterization of Some Metal Complexes of [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1H-pyrazol-4-ylcarbamothioyl) benzamide]', Alustath, 22(96), pp. 49-62.
M. Sarhan, B., of Education for Pure Sciences, C., of Education- Iraq, M., Ibn-AL-Haitham, , J. Waheed Department of Chemistry, E., of Baghdad Awf A.R. Ahmed Teacher, U. Synthesis and Characterization of Some Metal Complexes of [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1H-pyrazol-4-ylcarbamothioyl) benzamide]. Alustath, 2016; 22(96): 49-62.

Synthesis and Characterization of Some Metal Complexes of [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1H-pyrazol-4-ylcarbamothioyl) benzamide]

journal of the college of basic education
Article 1, Volume 22, Issue 96, December 2016, Pages 49-62
Authors
Basima M. Sarhan; College of Education for Pure Sciences; Ministry of Education- Iraq; ; Enass J. Waheed Department of Chemistry; University of Baghdad Awf A.R. Ahmed Teacher
Abstract
Abstract
A new ligand [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylcarb amothioyl) benzamide] (CAP) was synthesized by reaction of P-ChloroBenzoyl isothio cyanate with 4-aminoantipyrine,The ligand was characterized by micro elemental analysis C.H.N.S.,FT-IR,UV-Vis and1H-13CNMR spectra, some transition metals complex of this ligand were prepared and characterized by FT-IR, UV-Vis spectra, conductivity measurements, magnetic susceptibility and atomic absorption. From the obtained results the molecular formula of all prepared complexes were [M(CAP)2(H2O)2]Cl2(M+2 =Mn, Co, Ni, Cu, Zn, Cd and Hg),the proposed geometrical structure for all complexes were octahedral.
Key Word :4-Aminoantipyrine, P-ChloroBenzoyl isothiocyanate, complexes.
Keywords
Synthesis and Characterization of Some Metal Complexes of
Statistics
Article View: 178
PDF Download: 135


Journal Management System. Powered by ejournalplus.com