Synthesis And Characterization Of Some New Metals Complexes Of [N-(3-acetylphenylcarbamothioyl)-4-methoxybenzamide] | ||
| Diyala Journal For Pure Science | ||
| Article 1, Volume 12, Issue 1, February 2016, Pages 28-42 | ||
| Authors | ||
| Enass J. Waheed; Sajid M. Lateef; Basima M. Sarhan | ||
| Abstract | ||
| A new ligand [N-(3-acetylphenylcarbamothioyl)-4-methoxybenzamide](MAA) was synthesized by reaction of 4-methoxybenzoylisothiocyanate with 3-aminoacetophenone,The ligand was characterized by elemental microanalysis C.H.N.S, FT-IR, UV-Vis and 1H,13C- NMR spectra, some transition metals complexes of this ligand were prepared and characterized by FT-IR, UV-Vis spectra, conductivity measurements, magnetic susceptibility and atomic absorption, From obtained results the molecular formula of all prepared complexes were [M(MAA)2(H2O)2]Cl2 (M+2 =Mn, Co, Ni, Cu, Zn, Cd and Hg),the proposed geometrical structure for all complexes were octahedral. | ||
| Keywords | ||
| Aminoacetophenon; methoxybenzoylisothiocyanate; complexes | ||
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