Synthesis, Characterization and Chromatographic Study of Naphthol Derivatives | ||
| Journals kufa for chamical | ||
| Article 1, Volume 2, Issue 1, December 2016, Pages 18-31 | ||
| Author | ||
| Kasim Kadhim Alasedi | ||
| Abstract | ||
| A series of naphthol derivatives were synthesized from azo compound (A) and schiff bases compounds (B1-B6). The synthesized compounds structures are characterized by melting point, thin layer chromatography, CHN- analysis, FTIR, 1HNMR spectra, and13CNMR. In general, the order of elution, resolution and thermodynamic parameters of (A) and (B1-B6) on various liquid stationary phases (DN-1, FS-Bp10, DP5-S25, and OV-17) were discussed. The researcher found that the normal chromatographic behavior of specific retention volume Vgₒ of naphthol derivatives decreases by the increase of temperature of liquid stationary phases. | ||
| Keywords | ||
| naphthol derivatives; synthesis; gas chromatography; liquid stationary phase; temperature | ||
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