Synthesis and Characterization of Multishapes of Fe3O4 Nanoparticle by Solve-Hydrothermal Method Using Microwave Radiation | ||
| Baghdad Science Journal | ||
| Article 1, Volume 13, Issue 2, July 2016, Pages 331-339 | ||
| Authors | ||
| Ahlam Jameel Abdulghani; Waleed Madhloom Al-Ogedy | ||
| Abstract | ||
| Iron oxide(Fe3O4) nanoparticles of different sizes and shapes were synthesized by solve-hydrothermal reaction assisted by microwave irradiation using ferrous ammonium sulfate as a metal precursor, oleic acid as dispersing agent, ethanol as reducing agent and NaOH as precipitating agent at pH=12. The synthesized Fe3O4 nano particles were characterized by X-ray diffraction (XRD), FTIR and thermal analysis TG-DTG. Sizes and shapes of Fe3O4 nanoparticles were characterized by Scanning Electron Microscopy (SEM), and atomic force microscopy (AFM). | ||
| Keywords | ||
| Magnetite; microwave; oleic acid; SEM; AFM | ||
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